Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties

The solid state of samples (crystal, paracrystal, nanocrystal, amorphous), the main features of nanoobjects, their dimensional hierarchy and peculiarities of properties are considered. The main methods of studying the сomposition, substructure and microstructure characteristics of nanosized compound...

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Main Author: G. M. Kuzmicheva
Format: Article
Language:Russian
Published: MIREA - Russian Technological University 2015-12-01
Series:Тонкие химические технологии
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Online Access:https://www.finechem-mirea.ru/jour/article/view/265
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author G. M. Kuzmicheva
author_facet G. M. Kuzmicheva
author_sort G. M. Kuzmicheva
collection DOAJ
description The solid state of samples (crystal, paracrystal, nanocrystal, amorphous), the main features of nanoobjects, their dimensional hierarchy and peculiarities of properties are considered. The main methods of studying the сomposition, substructure and microstructure characteristics of nanosized compounds are proved. The basic method is X-ray study with specific effects on a diffraction picture. By the example of samples with anatase and η-phase structures obtained by the sulfate method the results of a complex of techniques (wide-angle and small-angle X-ray diffraction, synchrotron radiation, low temperature absorption of nitrogen, IR-spectroscopy, Raman spectroscopy) for the determination of the composition and structure of nanoparticles and their functional characteristics are shown. A relationship of some characteristics and preparation conditions of samples with parameters of the adsorption and photocatalytic properties is found.
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publisher MIREA - Russian Technological University
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series Тонкие химические технологии
spelling doaj-art-f99efea6be66452d88b49ebb8c9cd8e62025-08-04T10:19:37ZrusMIREA - Russian Technological UniversityТонкие химические технологии2410-65932686-75752015-12-01106536259Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. PropertiesG. M. Kuzmicheva0Moscow Technological University (Institute of Fine Chemical Technologies), 86, Vernadskogo pr., Moscow 119571The solid state of samples (crystal, paracrystal, nanocrystal, amorphous), the main features of nanoobjects, their dimensional hierarchy and peculiarities of properties are considered. The main methods of studying the сomposition, substructure and microstructure characteristics of nanosized compounds are proved. The basic method is X-ray study with specific effects on a diffraction picture. By the example of samples with anatase and η-phase structures obtained by the sulfate method the results of a complex of techniques (wide-angle and small-angle X-ray diffraction, synchrotron radiation, low temperature absorption of nitrogen, IR-spectroscopy, Raman spectroscopy) for the determination of the composition and structure of nanoparticles and their functional characteristics are shown. A relationship of some characteristics and preparation conditions of samples with parameters of the adsorption and photocatalytic properties is found.https://www.finechem-mirea.ru/jour/article/view/265nanoobjects, titanium(iv) oxides, anatase, η-phase, sulfate method, composition, structure, adsorption, photocatalysis.
spellingShingle G. M. Kuzmicheva
Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties
Тонкие химические технологии
nanoobjects, titanium(iv) oxides, anatase, η-phase, sulfate method, composition, structure, adsorption, photocatalysis.
title Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties
title_full Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties
title_fullStr Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties
title_full_unstemmed Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties
title_short Nanosized phases with titanium(IV) oxides. Preparation. Characterisation. Properties
title_sort nanosized phases with titanium iv oxides preparation characterisation properties
topic nanoobjects, titanium(iv) oxides, anatase, η-phase, sulfate method, composition, structure, adsorption, photocatalysis.
url https://www.finechem-mirea.ru/jour/article/view/265
work_keys_str_mv AT gmkuzmicheva nanosizedphaseswithtitaniumivoxidespreparationcharacterisationproperties