Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT

In this work, the 3D pore structure of pristine and oxidized IG-110 nuclear graphite was studied using X-ray micro-Computed Tomography (XCT). The results revealed a nonuniform oxidation profile in the bulk sample at 650 °C. A comprehensive methodology was developed to quantitatively characterize the...

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Main Authors: Xu Qiao, Guma Yeli, Shasha Lv, Zhengcao Li, Zhou Zhou
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425015649
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author Xu Qiao
Guma Yeli
Shasha Lv
Zhengcao Li
Zhou Zhou
author_facet Xu Qiao
Guma Yeli
Shasha Lv
Zhengcao Li
Zhou Zhou
author_sort Xu Qiao
collection DOAJ
description In this work, the 3D pore structure of pristine and oxidized IG-110 nuclear graphite was studied using X-ray micro-Computed Tomography (XCT). The results revealed a nonuniform oxidation profile in the bulk sample at 650 °C. A comprehensive methodology was developed to quantitatively characterize the complex pore structure, incorporating analysis of pore size distribution, morphology, fractal characteristics and two-point autocorrelation function based on the CT images. The findings demonstrated that both porosity and fractal dimension increased after oxidation. Furthermore, 2D image analysis provided a depth-dependent characterization of the oxidation profile highlighting significant variations in the surface and internal regions. The results underscore the potential of fractality as a comprehensive measure of porosity and structure inhomogeneity, offering additional parameters for a more quantitative description of the nuclear graphite microstructure.
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institution Matheson Library
issn 2238-7854
language English
publishDate 2025-07-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj-art-d37f990b1df54a03833a4b3b5cce972f2025-06-28T05:30:16ZengElsevierJournal of Materials Research and Technology2238-78542025-07-013723932405Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CTXu Qiao0Guma Yeli1Shasha Lv2Zhengcao Li3Zhou Zhou4Center for Neutron Science and Technology, Guangdong Provincial Key Laboratory of Magnetoelectric Physics and Devices, School of Physics, Sun Yat-sen University, Guangzhou, 510275, ChinaInstitute of Nuclear & New Energy Technology, Tsinghua University, Beijing, 100084, ChinaKey Laboratory of Beam Technology, Ministry of Education, College of Nuclear Science and Technology, Beijing Normal University, Beijing, 100875, ChinaKey Laboratory of Advanced Materials (MOE), School of Materials Science and Engineering, Tsinghua University, Beijing, 100084, ChinaCenter for Neutron Science and Technology, Guangdong Provincial Key Laboratory of Magnetoelectric Physics and Devices, School of Physics, Sun Yat-sen University, Guangzhou, 510275, China; Corresponding author.In this work, the 3D pore structure of pristine and oxidized IG-110 nuclear graphite was studied using X-ray micro-Computed Tomography (XCT). The results revealed a nonuniform oxidation profile in the bulk sample at 650 °C. A comprehensive methodology was developed to quantitatively characterize the complex pore structure, incorporating analysis of pore size distribution, morphology, fractal characteristics and two-point autocorrelation function based on the CT images. The findings demonstrated that both porosity and fractal dimension increased after oxidation. Furthermore, 2D image analysis provided a depth-dependent characterization of the oxidation profile highlighting significant variations in the surface and internal regions. The results underscore the potential of fractality as a comprehensive measure of porosity and structure inhomogeneity, offering additional parameters for a more quantitative description of the nuclear graphite microstructure.http://www.sciencedirect.com/science/article/pii/S2238785425015649Nuclear graphiteOxidationMicrostructureX-ray computed tomographyFractal
spellingShingle Xu Qiao
Guma Yeli
Shasha Lv
Zhengcao Li
Zhou Zhou
Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
Journal of Materials Research and Technology
Nuclear graphite
Oxidation
Microstructure
X-ray computed tomography
Fractal
title Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
title_full Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
title_fullStr Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
title_full_unstemmed Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
title_short Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
title_sort fractal analysis of pore structure of ig 110 nuclear graphite using x ray micro ct
topic Nuclear graphite
Oxidation
Microstructure
X-ray computed tomography
Fractal
url http://www.sciencedirect.com/science/article/pii/S2238785425015649
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AT shashalv fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct
AT zhengcaoli fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct
AT zhouzhou fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct