Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT
In this work, the 3D pore structure of pristine and oxidized IG-110 nuclear graphite was studied using X-ray micro-Computed Tomography (XCT). The results revealed a nonuniform oxidation profile in the bulk sample at 650 °C. A comprehensive methodology was developed to quantitatively characterize the...
Saved in:
Main Authors: | , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Elsevier
2025-07-01
|
Series: | Journal of Materials Research and Technology |
Subjects: | |
Online Access: | http://www.sciencedirect.com/science/article/pii/S2238785425015649 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
_version_ | 1839648821930360832 |
---|---|
author | Xu Qiao Guma Yeli Shasha Lv Zhengcao Li Zhou Zhou |
author_facet | Xu Qiao Guma Yeli Shasha Lv Zhengcao Li Zhou Zhou |
author_sort | Xu Qiao |
collection | DOAJ |
description | In this work, the 3D pore structure of pristine and oxidized IG-110 nuclear graphite was studied using X-ray micro-Computed Tomography (XCT). The results revealed a nonuniform oxidation profile in the bulk sample at 650 °C. A comprehensive methodology was developed to quantitatively characterize the complex pore structure, incorporating analysis of pore size distribution, morphology, fractal characteristics and two-point autocorrelation function based on the CT images. The findings demonstrated that both porosity and fractal dimension increased after oxidation. Furthermore, 2D image analysis provided a depth-dependent characterization of the oxidation profile highlighting significant variations in the surface and internal regions. The results underscore the potential of fractality as a comprehensive measure of porosity and structure inhomogeneity, offering additional parameters for a more quantitative description of the nuclear graphite microstructure. |
format | Article |
id | doaj-art-d37f990b1df54a03833a4b3b5cce972f |
institution | Matheson Library |
issn | 2238-7854 |
language | English |
publishDate | 2025-07-01 |
publisher | Elsevier |
record_format | Article |
series | Journal of Materials Research and Technology |
spelling | doaj-art-d37f990b1df54a03833a4b3b5cce972f2025-06-28T05:30:16ZengElsevierJournal of Materials Research and Technology2238-78542025-07-013723932405Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CTXu Qiao0Guma Yeli1Shasha Lv2Zhengcao Li3Zhou Zhou4Center for Neutron Science and Technology, Guangdong Provincial Key Laboratory of Magnetoelectric Physics and Devices, School of Physics, Sun Yat-sen University, Guangzhou, 510275, ChinaInstitute of Nuclear & New Energy Technology, Tsinghua University, Beijing, 100084, ChinaKey Laboratory of Beam Technology, Ministry of Education, College of Nuclear Science and Technology, Beijing Normal University, Beijing, 100875, ChinaKey Laboratory of Advanced Materials (MOE), School of Materials Science and Engineering, Tsinghua University, Beijing, 100084, ChinaCenter for Neutron Science and Technology, Guangdong Provincial Key Laboratory of Magnetoelectric Physics and Devices, School of Physics, Sun Yat-sen University, Guangzhou, 510275, China; Corresponding author.In this work, the 3D pore structure of pristine and oxidized IG-110 nuclear graphite was studied using X-ray micro-Computed Tomography (XCT). The results revealed a nonuniform oxidation profile in the bulk sample at 650 °C. A comprehensive methodology was developed to quantitatively characterize the complex pore structure, incorporating analysis of pore size distribution, morphology, fractal characteristics and two-point autocorrelation function based on the CT images. The findings demonstrated that both porosity and fractal dimension increased after oxidation. Furthermore, 2D image analysis provided a depth-dependent characterization of the oxidation profile highlighting significant variations in the surface and internal regions. The results underscore the potential of fractality as a comprehensive measure of porosity and structure inhomogeneity, offering additional parameters for a more quantitative description of the nuclear graphite microstructure.http://www.sciencedirect.com/science/article/pii/S2238785425015649Nuclear graphiteOxidationMicrostructureX-ray computed tomographyFractal |
spellingShingle | Xu Qiao Guma Yeli Shasha Lv Zhengcao Li Zhou Zhou Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT Journal of Materials Research and Technology Nuclear graphite Oxidation Microstructure X-ray computed tomography Fractal |
title | Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT |
title_full | Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT |
title_fullStr | Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT |
title_full_unstemmed | Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT |
title_short | Fractal analysis of pore structure of IG-110 nuclear graphite using X-ray micro-CT |
title_sort | fractal analysis of pore structure of ig 110 nuclear graphite using x ray micro ct |
topic | Nuclear graphite Oxidation Microstructure X-ray computed tomography Fractal |
url | http://www.sciencedirect.com/science/article/pii/S2238785425015649 |
work_keys_str_mv | AT xuqiao fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct AT gumayeli fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct AT shashalv fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct AT zhengcaoli fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct AT zhouzhou fractalanalysisofporestructureofig110nucleargraphiteusingxraymicroct |