Solid-state synthesis of pure belite polymorphs

The solid-state synthesis of pure belite polymorphs is still not described in detail. The study of this issue is important for understanding modification transformations, especially between beta and gamma modifications. In this paper, the two-step firing procedure was used to study belite transform...

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Main Authors: Michal Křištof, Andrea Jančíková, Karel Dvořák
Format: Article
Language:English
Published: Czech Technical University in Prague 2025-07-01
Series:Acta Polytechnica CTU Proceedings
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Online Access:https://ojs.cvut.cz/ojs/index.php/APP/article/view/10742
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author Michal Křištof
Andrea Jančíková
Karel Dvořák
author_facet Michal Křištof
Andrea Jančíková
Karel Dvořák
author_sort Michal Křištof
collection DOAJ
description The solid-state synthesis of pure belite polymorphs is still not described in detail. The study of this issue is important for understanding modification transformations, especially between beta and gamma modifications. In this paper, the two-step firing procedure was used to study belite transformations. The first firing step was designed to produce samples with high content of γ-C2S. These samples were fired again and successfully transformed into β-C2S without any additional chemicals. In addition to firing parameters, the effect of particle size was also monitored. The experiment succeeded in creating a sample containing 64 % gamma belite in total and also a sample containing a total of 90 % of beta belite.
format Article
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issn 2336-5382
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publishDate 2025-07-01
publisher Czech Technical University in Prague
record_format Article
series Acta Polytechnica CTU Proceedings
spelling doaj-art-7dd6d5fc1cb54fd5aa71576aa9f6449d2025-07-15T11:18:08ZengCzech Technical University in PragueActa Polytechnica CTU Proceedings2336-53822025-07-015310.14311/APP.2025.53.0049Solid-state synthesis of pure belite polymorphsMichal Křištof0Andrea Jančíková1Karel Dvořák2Brno University of Technology, Faculty of Civil Engineering, Veveří 331/95, 602 00 Brno, Czech RepublicBrno University of Technology, Faculty of Civil Engineering, Veveří 331/95, 602 00 Brno, Czech RepublicBrno University of Technology, Faculty of Civil Engineering, Veveří 331/95, 602 00 Brno, Czech Republic The solid-state synthesis of pure belite polymorphs is still not described in detail. The study of this issue is important for understanding modification transformations, especially between beta and gamma modifications. In this paper, the two-step firing procedure was used to study belite transformations. The first firing step was designed to produce samples with high content of γ-C2S. These samples were fired again and successfully transformed into β-C2S without any additional chemicals. In addition to firing parameters, the effect of particle size was also monitored. The experiment succeeded in creating a sample containing 64 % gamma belite in total and also a sample containing a total of 90 % of beta belite. https://ojs.cvut.cz/ojs/index.php/APP/article/view/10742clinkerbelitepolymorphism
spellingShingle Michal Křištof
Andrea Jančíková
Karel Dvořák
Solid-state synthesis of pure belite polymorphs
Acta Polytechnica CTU Proceedings
clinker
belite
polymorphism
title Solid-state synthesis of pure belite polymorphs
title_full Solid-state synthesis of pure belite polymorphs
title_fullStr Solid-state synthesis of pure belite polymorphs
title_full_unstemmed Solid-state synthesis of pure belite polymorphs
title_short Solid-state synthesis of pure belite polymorphs
title_sort solid state synthesis of pure belite polymorphs
topic clinker
belite
polymorphism
url https://ojs.cvut.cz/ojs/index.php/APP/article/view/10742
work_keys_str_mv AT michalkristof solidstatesynthesisofpurebelitepolymorphs
AT andreajancikova solidstatesynthesisofpurebelitepolymorphs
AT kareldvorak solidstatesynthesisofpurebelitepolymorphs