Optimization of nanostructured/nano sized rice husk ash preparation

The objective of the study is developing a procedure for production and characterization of rice husk ash (RHA). The effects of rice husk (RH) amount, burning/cooling conditions combined with stirring on producing of RHA with amorphous silica, highest SiO2, lowest loss on ignition (LOI), uniform par...

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Main Authors: Medhat Mostafa, Hamdy Salah, Amro B. Saddek, Nabila Shehata
Format: Article
Language:English
Published: University of Baghdad, College of Science for Women 2020-09-01
Series:مجلة بغداد للعلوم
Subjects:
Online Access:http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/3835
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author Medhat Mostafa
Hamdy Salah
Amro B. Saddek
Nabila Shehata
author_facet Medhat Mostafa
Hamdy Salah
Amro B. Saddek
Nabila Shehata
author_sort Medhat Mostafa
collection DOAJ
description The objective of the study is developing a procedure for production and characterization of rice husk ash (RHA). The effects of rice husk (RH) amount, burning/cooling conditions combined with stirring on producing of RHA with amorphous silica, highest SiO2, lowest loss on ignition (LOI), uniform particle shape distribution and nano structured size have been studied. It is concluded that the best amount is 20 g RH in 125 ml evaporating dish Porcelain with burning for 2 h at temperature 700 °C combined with cooling three times during burning to produce RHA with amorphous silica, SiO2 90.78% and LOI 1.73%. On the other hand, cooling and stirring times affect the variation of nano structured size and particle shape distribution. However, no crystalline phases were found in RHA in all cases. Results proved that the Attritor ball mill was more suitable than vibration disk mill for pulverizing nano structured RHA with 50% of particle size (D50) lower than 45 mm and 99 % of particle size (D99) lower than 144 mm to nanosized RHA with D50 lower than 36 nm and D99 lower than 57 nm by grinding time 8.16 min to every 1 g RHA without changes in morphousity of silica.
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series مجلة بغداد للعلوم
spelling doaj-art-42f208e52f7c4650ba1d0caac61a6bb52025-08-02T06:25:58ZengUniversity of Baghdad, College of Science for Womenمجلة بغداد للعلوم2078-86652411-79862020-09-01173(Suppl.)10.21123/bsj.2020.17.3(Suppl.).0953Optimization of nanostructured/nano sized rice husk ash preparationMedhat Mostafa0Hamdy Salah1Amro B. Saddek2Nabila Shehata3Assiut Cement Company, CEMEX EgyptMinia White Cement Plant, Heidelberg Cement GroupFaculty of Engineering, Beni-Suef UniversityFaculty of Postgraduate studies for Advanced Science, Beni-Suef UniversityThe objective of the study is developing a procedure for production and characterization of rice husk ash (RHA). The effects of rice husk (RH) amount, burning/cooling conditions combined with stirring on producing of RHA with amorphous silica, highest SiO2, lowest loss on ignition (LOI), uniform particle shape distribution and nano structured size have been studied. It is concluded that the best amount is 20 g RH in 125 ml evaporating dish Porcelain with burning for 2 h at temperature 700 °C combined with cooling three times during burning to produce RHA with amorphous silica, SiO2 90.78% and LOI 1.73%. On the other hand, cooling and stirring times affect the variation of nano structured size and particle shape distribution. However, no crystalline phases were found in RHA in all cases. Results proved that the Attritor ball mill was more suitable than vibration disk mill for pulverizing nano structured RHA with 50% of particle size (D50) lower than 45 mm and 99 % of particle size (D99) lower than 144 mm to nanosized RHA with D50 lower than 36 nm and D99 lower than 57 nm by grinding time 8.16 min to every 1 g RHA without changes in morphousity of silica.http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/3835Grinding, Nano Structured, Nano Sized, Optimization, Rice Husk Ash
spellingShingle Medhat Mostafa
Hamdy Salah
Amro B. Saddek
Nabila Shehata
Optimization of nanostructured/nano sized rice husk ash preparation
مجلة بغداد للعلوم
Grinding, Nano Structured, Nano Sized, Optimization, Rice Husk Ash
title Optimization of nanostructured/nano sized rice husk ash preparation
title_full Optimization of nanostructured/nano sized rice husk ash preparation
title_fullStr Optimization of nanostructured/nano sized rice husk ash preparation
title_full_unstemmed Optimization of nanostructured/nano sized rice husk ash preparation
title_short Optimization of nanostructured/nano sized rice husk ash preparation
title_sort optimization of nanostructured nano sized rice husk ash preparation
topic Grinding, Nano Structured, Nano Sized, Optimization, Rice Husk Ash
url http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/3835
work_keys_str_mv AT medhatmostafa optimizationofnanostructurednanosizedricehuskashpreparation
AT hamdysalah optimizationofnanostructurednanosizedricehuskashpreparation
AT amrobsaddek optimizationofnanostructurednanosizedricehuskashpreparation
AT nabilashehata optimizationofnanostructurednanosizedricehuskashpreparation