Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles

Co₃O₄ nanoparticles were synthesized using a green method and applied for photocatalytic degradation of tetracycline (TC) in aqueous solution. These nanoparticles were characterized using various techniques, including X-ray Diffraction (XRD), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-...

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Main Authors: Omar Mohammed, Ali Naghipour, Saeid Taghavi Fardood
Format: Article
Language:English
Published: Iranian Chemical Society 2025-04-01
Series:Nanochemistry Research
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Online Access:http://www.nanochemres.org/article_216617_8e651bebdc6c2d7c08c8612d0d382d84.pdf
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author Omar Mohammed
Ali Naghipour
Saeid Taghavi Fardood
author_facet Omar Mohammed
Ali Naghipour
Saeid Taghavi Fardood
author_sort Omar Mohammed
collection DOAJ
description Co₃O₄ nanoparticles were synthesized using a green method and applied for photocatalytic degradation of tetracycline (TC) in aqueous solution. These nanoparticles were characterized using various techniques, including X-ray Diffraction (XRD), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS), Transmission Electron Microscopy (TEM), Brunauer–Emmett–Teller (BET) analysis, Field Emission Scanning Electron Microscopy (FESEM), and Energy-Dispersive X-ray Spectroscopy (EDS) mapping techniques. The XRD pattern also revealed high crystallinity of the Co₃O₄ nanoparticles and confirmed their cubic crystal structure with a crystallite size of about 20 nm, as determined by the Scherrer equation. Further analysis of the sample by TEM indicated that the particle size was approximately 35 nm. The UV-Vis DRS analysis showed a band gap of 2.09 eV, supporting its potential as an effective photocatalyst. The BET analysis demonstrated that the surface area of the Co₃O₄ nanoparticles was 14.34 m²/g. The Co₃O₄ nanoparticles demonstrated strong photocatalytic activity, achieving 95% degradation of tetracycline within 3 hours under visible light at room temperature.
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spelling doaj-art-3e3564c17c96477bb9a4aa5f85ff1b6d2025-07-23T12:59:18ZengIranian Chemical SocietyNanochemistry Research2538-42792423-818X2025-04-0110223323910.22036/NCR.2025.02.08216617Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 NanoparticlesOmar Mohammed0Ali Naghipour1Saeid Taghavi Fardood2Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.Co₃O₄ nanoparticles were synthesized using a green method and applied for photocatalytic degradation of tetracycline (TC) in aqueous solution. These nanoparticles were characterized using various techniques, including X-ray Diffraction (XRD), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS), Transmission Electron Microscopy (TEM), Brunauer–Emmett–Teller (BET) analysis, Field Emission Scanning Electron Microscopy (FESEM), and Energy-Dispersive X-ray Spectroscopy (EDS) mapping techniques. The XRD pattern also revealed high crystallinity of the Co₃O₄ nanoparticles and confirmed their cubic crystal structure with a crystallite size of about 20 nm, as determined by the Scherrer equation. Further analysis of the sample by TEM indicated that the particle size was approximately 35 nm. The UV-Vis DRS analysis showed a band gap of 2.09 eV, supporting its potential as an effective photocatalyst. The BET analysis demonstrated that the surface area of the Co₃O₄ nanoparticles was 14.34 m²/g. The Co₃O₄ nanoparticles demonstrated strong photocatalytic activity, achieving 95% degradation of tetracycline within 3 hours under visible light at room temperature.http://www.nanochemres.org/article_216617_8e651bebdc6c2d7c08c8612d0d382d84.pdfco3o4 npsgreen synthesistetracycline degradationphotocatalytic activity
spellingShingle Omar Mohammed
Ali Naghipour
Saeid Taghavi Fardood
Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
Nanochemistry Research
co3o4 nps
green synthesis
tetracycline degradation
photocatalytic activity
title Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
title_full Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
title_fullStr Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
title_full_unstemmed Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
title_short Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
title_sort green synthesis characterization and photocatalytic activity of co3o4 nanoparticles
topic co3o4 nps
green synthesis
tetracycline degradation
photocatalytic activity
url http://www.nanochemres.org/article_216617_8e651bebdc6c2d7c08c8612d0d382d84.pdf
work_keys_str_mv AT omarmohammed greensynthesischaracterizationandphotocatalyticactivityofco3o4nanoparticles
AT alinaghipour greensynthesischaracterizationandphotocatalyticactivityofco3o4nanoparticles
AT saeidtaghavifardood greensynthesischaracterizationandphotocatalyticactivityofco3o4nanoparticles