Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles
Co₃O₄ nanoparticles were synthesized using a green method and applied for photocatalytic degradation of tetracycline (TC) in aqueous solution. These nanoparticles were characterized using various techniques, including X-ray Diffraction (XRD), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-...
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Iranian Chemical Society
2025-04-01
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Series: | Nanochemistry Research |
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Online Access: | http://www.nanochemres.org/article_216617_8e651bebdc6c2d7c08c8612d0d382d84.pdf |
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author | Omar Mohammed Ali Naghipour Saeid Taghavi Fardood |
author_facet | Omar Mohammed Ali Naghipour Saeid Taghavi Fardood |
author_sort | Omar Mohammed |
collection | DOAJ |
description | Co₃O₄ nanoparticles were synthesized using a green method and applied for photocatalytic degradation of tetracycline (TC) in aqueous solution. These nanoparticles were characterized using various techniques, including X-ray Diffraction (XRD), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS), Transmission Electron Microscopy (TEM), Brunauer–Emmett–Teller (BET) analysis, Field Emission Scanning Electron Microscopy (FESEM), and Energy-Dispersive X-ray Spectroscopy (EDS) mapping techniques. The XRD pattern also revealed high crystallinity of the Co₃O₄ nanoparticles and confirmed their cubic crystal structure with a crystallite size of about 20 nm, as determined by the Scherrer equation. Further analysis of the sample by TEM indicated that the particle size was approximately 35 nm. The UV-Vis DRS analysis showed a band gap of 2.09 eV, supporting its potential as an effective photocatalyst. The BET analysis demonstrated that the surface area of the Co₃O₄ nanoparticles was 14.34 m²/g. The Co₃O₄ nanoparticles demonstrated strong photocatalytic activity, achieving 95% degradation of tetracycline within 3 hours under visible light at room temperature. |
format | Article |
id | doaj-art-3e3564c17c96477bb9a4aa5f85ff1b6d |
institution | Matheson Library |
issn | 2538-4279 2423-818X |
language | English |
publishDate | 2025-04-01 |
publisher | Iranian Chemical Society |
record_format | Article |
series | Nanochemistry Research |
spelling | doaj-art-3e3564c17c96477bb9a4aa5f85ff1b6d2025-07-23T12:59:18ZengIranian Chemical SocietyNanochemistry Research2538-42792423-818X2025-04-0110223323910.22036/NCR.2025.02.08216617Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 NanoparticlesOmar Mohammed0Ali Naghipour1Saeid Taghavi Fardood2Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.Co₃O₄ nanoparticles were synthesized using a green method and applied for photocatalytic degradation of tetracycline (TC) in aqueous solution. These nanoparticles were characterized using various techniques, including X-ray Diffraction (XRD), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS), Transmission Electron Microscopy (TEM), Brunauer–Emmett–Teller (BET) analysis, Field Emission Scanning Electron Microscopy (FESEM), and Energy-Dispersive X-ray Spectroscopy (EDS) mapping techniques. The XRD pattern also revealed high crystallinity of the Co₃O₄ nanoparticles and confirmed their cubic crystal structure with a crystallite size of about 20 nm, as determined by the Scherrer equation. Further analysis of the sample by TEM indicated that the particle size was approximately 35 nm. The UV-Vis DRS analysis showed a band gap of 2.09 eV, supporting its potential as an effective photocatalyst. The BET analysis demonstrated that the surface area of the Co₃O₄ nanoparticles was 14.34 m²/g. The Co₃O₄ nanoparticles demonstrated strong photocatalytic activity, achieving 95% degradation of tetracycline within 3 hours under visible light at room temperature.http://www.nanochemres.org/article_216617_8e651bebdc6c2d7c08c8612d0d382d84.pdfco3o4 npsgreen synthesistetracycline degradationphotocatalytic activity |
spellingShingle | Omar Mohammed Ali Naghipour Saeid Taghavi Fardood Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles Nanochemistry Research co3o4 nps green synthesis tetracycline degradation photocatalytic activity |
title | Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles |
title_full | Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles |
title_fullStr | Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles |
title_full_unstemmed | Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles |
title_short | Green Synthesis, Characterization and Photocatalytic Activity of Co3O4 Nanoparticles |
title_sort | green synthesis characterization and photocatalytic activity of co3o4 nanoparticles |
topic | co3o4 nps green synthesis tetracycline degradation photocatalytic activity |
url | http://www.nanochemres.org/article_216617_8e651bebdc6c2d7c08c8612d0d382d84.pdf |
work_keys_str_mv | AT omarmohammed greensynthesischaracterizationandphotocatalyticactivityofco3o4nanoparticles AT alinaghipour greensynthesischaracterizationandphotocatalyticactivityofco3o4nanoparticles AT saeidtaghavifardood greensynthesischaracterizationandphotocatalyticactivityofco3o4nanoparticles |